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The process according to any one of the preceding embodiments, wherein the GLP-1 peptide is selected from semaglutide or l\l27-[2-[2-[2-[[2-[2-[2-[[(4S)-4-carboxy-4-[10- (4-carboxyphenoxy)decanoylamino]butanoyl]amino]ethoxy]ethoxy] acetyl]amino]ethoxy]ethoxy]acetyl], l\l36-[2-[2-[2-[[2-[2-[2-[[(4S)-4-carboxy-4-[10-(4- carboxyphenoxy)decanoylamino]butanoyl]amino]ethoxy]ethoxy]acetyl]amino]ethoxy]e thoxy]acetyl]-[Aib8,Glu22,Arg26,Lys27,Glu30,Arg34,Lys36]-GLP-1-(7-37)-peptidyl- Glu-Gly (Compound A)

Final disulfide bond formation was conducted after complete deprotection using hydrogen peroxide