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Fmoc-Gln(Trt)-Ala-Ala-Lys(C18 diacid mono-t-butyl-Y-Glu(AEEA-AEEA)-OtBu)-Glu (OtBu)- Phe-Ile-Ala-Trp(Boc)-OH (fragment-4) The present invention provides a solid phase peptide process for the preparation of Fmoc-Gln(Trt) Ala-Ala-Lys(Cl 8 diacid mono-t-butyl-y-Glu(AEEA-AEEA)-OtBu)-Glu(OtBu)-Phe-Ile-Ala-Trp (Boc)-OH of fragment-4 which comprises: a) anchoring Fmoc-Trp(Boc)-OH to a resin in presence of a coupling agent

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